Search results for "Complexing agents"

showing 2 items of 2 documents

A simple method to fabricate high-performance nanostructured WO3 photocatalysts with adjusted morphology in the presence of complexing agents

2017

[EN] The rich and complex chemistry of tungsten was employed to synthesize innovative WO3 nanoplatelets/nanosheets by simple anodization in acidic electrolytes containing different concentrations of complexing agents or ligands, namely F- and H2O2. The morphological and photoelectrochemical properties of these nanostructures were characterized. The best of these nanostructures generated stable photocurrent densities of ca. 1.8 mA cm(-2) at relatively low bias potentials (for WO3) of 0.7 V-Ag/AgCl under simulated solar irradiation, which can be attributed to a very high active surface area. This work demonstrates that the morphology and dimensions of these nanostructures, as well as their ph…

Complexing agentsNanostructureMaterials sciencechemistry.chemical_elementNanotechnology02 engineering and technologyElectrolyteTungsten010402 general chemistryElectrochemistry01 natural sciencesINGENIERIA QUIMICACatalysisSynthesislcsh:TA401-492General Materials SciencePhotocatalysisPhotocurrentNanoestructuresAnodizingMechanical EngineeringHydrogen peroxide021001 nanoscience & nanotechnologyWO3 nanostructures0104 chemical sciencesElectroquímicachemistryMechanics of MaterialsPhotocatalysislcsh:Materials of engineering and construction. Mechanics of materialsAnodization0210 nano-technology
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Customized WO3 nanoplatelets as visible-light photoelectrocatalyst for the degradation of a recalcitrant model organic compound (methyl orange)

2018

[EN] WO3 nanoplatelets have been synthesized by electrochemical anodization in acidic electrolytes containing two different complexing agents: fluorides and hydrogen peroxide. The influence of the morphology and size of these nanoplatelets on their photoelectrocatalytic performance has been studied following the degradation of a model organic recalcitrant compound, such as methyl orange (MO). The effect of several supporting electrolytes on this photodegradation process has also been checked. The best MO decoloration was observed for nanoplatelets fabricated in the presence of low H2O2 concentrations, whose distribution and small size made them expose a very high surface area to the problem…

NanostructureComplexing agentsGeneral Chemical EngineeringGeneral Physics and Astronomy02 engineering and technologyElectrolyte010402 general chemistry01 natural sciencesOrganic compoundINGENIERIA QUIMICAchemistry.chemical_compoundMethyl orangeHydrogen peroxidePhotodegradationchemistry.chemical_classificationNanoestructuresAnodizingGeneral Chemistry021001 nanoscience & nanotechnologyWO3 nanostructures0104 chemical sciencesElectroquímicachemistryChemical engineeringMethyl orangePhotoelectrocatalysisAnodization0210 nano-technologyVisible spectrum
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